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News & updates
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How to Characterize (Oxygen/Nitrogen) Defects/Vacancies at Transition Metal Oxide?
I. XPS and XRD 1. Refrences 2. Typical Reasons for the Formation of OXygen Vacancies The formation of VO″ may be caused by the following factors: (i) the lattice O was oxidized to O2 during polarization and (ii) Se on the surface may be oxidized to Se element and peeled off, thus leading to oxygen…
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Water splitting
Oxygen Evolution Reaction References Mechanism of enhancement Case I: Dope V into CoP2[Angew. Chem.2022,134, e202116] the O XPS spectrum displays an obvious increased intensity of peak belonging to the adsorbed H2O (Figure 5h), suggesting the H2O adsorption ability is improved. Importantly, a new peak appears at 532.5 eV assigned to the oxygen vacancy,46 which often plays a…
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Electrochemical Alcohol Oxidation Reaction (AOR)
References 1. NonAqueous AOR 2. Aqueous AOR 2.1. References 2.2. Experiments 2.2.1. Preparing substrate 2.2.1. Preparing working electrode 2.2.3. Preparing electrolyte Electrolyte solutions used for oxygen evolution reaction (OER) experiments contained 1 M NaOH in water, and electrolyte solutions used for alcohol oxidation experiments (AOR) contained 1 M NaOH and 100 mM alcohol (EtOH, n-PrOH,…
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