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General Electrochemistry
References ElectroChemistry (EC) vs. PhotoElectroChemistry (PEC) In electrochemical N2 reduction, N2 reduction at the cathode is paired with water oxidation at the anode (Scheme 1a). The overall reaction is thermodynamically uphill, and therefore, an electrochemical N2 reduction cell requires an electrical energy input as in the case of an electrochemical water splitting cell. A photoelectrochemical…
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Preparation for Characterization
1. References 2. Brunaeur−Emmet−Teller (BET) The oxide samples were heated at 150 °C for 8–12 h to remove impurities, then immediately weighed, and transferred to the sample tube for measurement. The surface area was calculated with the Brunauer–Emmett–Teller (BET) method in the relative pressure range of 0.005–0.25 of adsorption data.[ACS Catal. 2023, 13, 1, 515–529]…
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Prepare working electrode
References 1. NonAqueous NITRR 2. Aqueous NITRR 2.1. References 2.2. For Electrochemical Catalyst 2.2.1. Preparing working electrode Material loaded on carbon cloth (1.0×1.0 cm2) were used as the working electrode. For the preparation of catalysts loaded on carbon cloth, the carbon cloth was first ultrasonically cleaned for several times in alternative baths of deionized water…
