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- 6:00 PM, Tuesday, July 21, 2024
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News & updates
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Synthetic Technique
Case 1: Cobalt Oxide Nanoparticles [prof. Joon T. Park’s group] Example 1: The fcc CoO solid nanoparallelepipeds, are reduced by the oleylamine surfactant to form fcc Co hollow nanoparallelepipeds A green slurry of [Co(acac)3] (0.10 g, 0.28 mmol) in neat oleylamine (9.24 mL) was heated at 135 °C for 5 min. Immediately after dissolution, the reaction mixture was flash-heated to 200 °C. After…
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X-ray diffraction
References Lattice Strain Formation through Spin-Coupled Shells of MoS2 on Mo2C for Bifunctional Oxygen Reduction and Oxygen Evolution Reaction Electrocatalysts Adv. Mater. Interfaces 2019, 6, 1900948 Calculate lattice strain Relative strain in MoS2 of core-shell structures is calculated by the Williamson-Hall method (W-H method) (Acta Metall. 1, 22-31 (1953)). W-H method based on the principle…
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X-ray Photoelectron Spectroscopy
Reference Modified Oxygen Defect Chemistry at Transition Metal Oxide Heterostructures Probed by Hard X-ray Photoelectron Spectroscopy and X-ray Diffraction I. Inorganic Chemistry Reference 1. XPS Why does XPS metal spectrum contain two main peaks, M 2p1/2 and M 2p3/2 ? They correspond to different spin–orbit couplings of metal (spin−orbital peaks) What does satellite peaks assign…
